Issue 30

A. Martín-Meizoso et alii, Frattura ed Integrità Strutturale, 30 (2014) 14-22; DOI: 10.3221/IGF-ESIS.30.03 15 Figure 1 : Mini-Tensile testpiece, instrumented with a strain gauge. M ATERIALS AND EXPERIMENTAL TECHNIQUES his work presents the characterization of a cut edge of a thick (25 mm) plate made of a steel of intermediate strength (S460M). This plate is cut by oxy-fuel gas (flame cut) under the standard industrial cutting conditions typical for heavy plates. From adjacent-to-the-cut region samples were obtained for metallography, hardness measurements and mini-tensile specimens. Metallographic samples were embedded in a conductive acrylic resin (Condufast). Afterwards the observation side is prepared by polishing with SiC papers until grade 1200 and it is further polished -to a mirror finish- by using velvet clothes with a diamond paste of 6 microns. Finally the samples are etched with 2% nital for 15 s and observed on an optical microscope (Leica MEF-4). Hardness profiles were carried out with a LECO M-400-G2, equipped with a Vickers’ pyramid and using an indentation load of 4.93 N (0.5 kg). Mini-Tensile probes were cut by Wire Electro-Discharge Machining (WEDM). Twelve prisms -with a dog-bone shape- were machined perpendicular to the cut edge. Four of them were obtained from the upper region of the cut (torch side), four from the middle thickness of the cut, and the other four from the lowest part of cut (flame exit and slag side). The middle sections of mini-tensiles are then located at 2.5 mm from the upper surface, at the middle (12.5 mm) and at 2.5 mm above the lower plate surface. Afterwards, these prisms are sliced into 300 microns sheets. These sheets are displaced by 150 microns among the different prisms, thus mini-tensiles are distributed with a resolution of 150 microns in distance from cut surface. Mini- tensiles are extracted with a longitudinal orientation (L) with respect to the plate rolling direction and their surfaces parallel to cut edge. According to literature [12-13], WEDM introduces residual stresses and affects to a depth of about 80 microns. In order to remove the effects of WEDM, 50 microns from each side of the test-piece are grinded away and the samples are then polished with SiC 1200 grade paper and velvet clothe with diamond paste of 6 microns. Test-pieces are not moved during polishing (at the automatic polishing machine: Struers) to provide a longitudinal polishing pattern, parallel to the future loading direction. The final test-piece thickness is 200 microns (nominally. It will be measured for each individual test- piece). The cut edge surface is not polished, but retained for the most superficial test-piece. This first mini-tensile test- piece is only polished at the inner surface (twice as hard -removing 100 microns for this side- to result in an identical final thickness of aprox. 200 microns). Fig. 1 shows a mini-tensile probe. Its basic dimensions are 20 mm in total length, 5 mm total width, 2.5 mm width in the reduced waist section and 0.2 mm thickness. To obtain accurate strain measurements, individual test-piece are instrumented with one strain gauge (HBM 1-LY11- 3/120 with a 5% of maximum strain). A San-Ei amplifier is used to record strain gauge elongations. Tensile tests are conducted at a ram speed of 0.1 mm/minute. For strains larger than a 5%, the ram position records are used (after correlation with the previous strain measurements obtained from the strain gauge). An electro-mechanical testing machine (Instron Mini 44) is used to carry out the mini-tensile tests. This testing machine has a load cell of ± 500 N. Test-piece heads are introduced into a slot machined at the ends of two volts. These slots are 300 microns thick. Then test-piece heads are glued in position with cyanoacrylate adhesive (Loctite), capillarity does the filling. Fig. 2 shows the experimental arrangement. T